Information card for entry 4323534

Structure parameters

• Formula: C25 H38 F12 N8 O5 P3 Re
• Calculated formula: C25 H38 F12 N8 O5 P3 Re
• Title of publication: Oxo Ligand Reactivity in the [ReO2L4]+ Complex of 1-Methylimidazole. Preparation and Crystal Structures of Salts Containing the ReOL43+ Core and Apical CH3O-, BF3O2-, and (CH3O)2PO2- Groups
• Authors of publication: Suzanne Bélanger; André L. Beauchamp
• Journal of publication: Inorganic Chemistry
• Year of publication: 1997
• Journal volume: 36
• Pages of publication: 3640 - 3647
• a: 14.165 ± 0.004 Å
• b: 13.052 ± 0.006 Å
• c: 20.931 ± 0.006 Å
• α: 90°
• β: 95.83 ± 0.02°
• γ: 90°
• Cell volume: 3850 ± 2 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0548
• Residual factor for significantly intense reflections: 0.0373
• Weighted residual factors for all reflections: 0.0903
• Weighted residual factors for significantly intense reflections: 0.0853
• Goodness-of-fit parameter for all reflections: 0.918
• Goodness-of-fit parameter for significantly intense reflections: 1.022
• Diffraction radiation wavelength: 1.54056 Å
• Diffraction radiation type: CopperKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No