Information card for entry 4323822

Structure parameters

• Chemical name: bis(diaquahydrogen) tris(2-aminoethyl)aminepotassium hexachlororuthenium(III)
• Formula: C6 H28 Cl6 K N4 O4 Ru
• Calculated formula: C6 H18 Cl6 K0.333333 N3.33333 O3.33333 Ru0.166667
• Title of publication: Syntheses and Crystal Structures of Ruthenium Complexes of 1,4,8,11-Tetraazacyclotetradecane, Tris(2-aminoethyl)amine (tren), and Bis(2-aminoethyl)(iminomethyl)amine. A Microporous Layered Structure Consisting of {[K(tren)]2[RuCl6]}nn- and {(H5O2)4[RuCl6]}nn+
• Authors of publication: Ken Sakai; Yasutaka Yamada; Taro Tsubomura
• Journal of publication: Inorganic Chemistry
• Year of publication: 1996
• Journal volume: 35
• Pages of publication: 3163 - 3172
• a: 10.254 ± 0.004 Å
• b: 10.254 Å
• c: 35.03 ± 0.01 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 3189.8 ± 1.5 ų
• Cell temperature: 293 K
• Ambient diffraction temperature: 293 K
• Number of distinct elements: 7
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for significantly intense reflections: 0.0504
• Weighted residual factors for significantly intense reflections: 0.0455
• Goodness-of-fit parameter for significantly intense reflections: 2.54
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No