Information card for entry 4323823

Structure parameters

• Chemical name: tris(2-aminoethyl)amine-oxalato-chloro-ruthenium(III) hydrochloric acid 3/2hydrate
• Formula: C8 H22 Cl2 N4 O5.5 Ru
• Calculated formula: C8 H19 Cl2 N4 O5.5 Ru
• Title of publication: Syntheses and Crystal Structures of Ruthenium Complexes of 1,4,8,11-Tetraazacyclotetradecane, Tris(2-aminoethyl)amine (tren), and Bis(2-aminoethyl)(iminomethyl)amine. A Microporous Layered Structure Consisting of {[K(tren)]2[RuCl6]}nn- and {(H5O2)4[RuCl6]}nn+
• Authors of publication: Ken Sakai; Yasutaka Yamada; Taro Tsubomura
• Journal of publication: Inorganic Chemistry
• Year of publication: 1996
• Journal volume: 35
• Pages of publication: 3163 - 3172
• a: 10.336 ± 0.002 Å
• b: 14.835 ± 0.002 Å
• c: 10.234 ± 0.001 Å
• α: 90.28 ± 0.01°
• β: 90.99 ± 0.01°
• γ: 92.07 ± 0.01°
• Cell volume: 1567.9 ± 0.4 ų
• Cell temperature: 296 K
• Ambient diffraction temperature: 296 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.037
• Weighted residual factors for significantly intense reflections: 0.0313
• Goodness-of-fit parameter for significantly intense reflections: 2.3
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No