Information card for entry 4323909

Structure parameters

• Chemical name: {trans-(Cl)([14]aneN~4~)RhH}~2~(ZnCl~4~)-dmso
• Formula: C22 H54 Cl6 N8 O Rh2 S Zn
• Calculated formula: C22 H56 Cl6 N8 O Rh2 S Zn
• SMILES: [RhH]123(Cl)[NH]4CCC[NH]1CC[NH]2CCC[NH]3CC4.[RhH]123(Cl)[NH]4CCC[NH]1CC[NH]2CCC[NH]3CC4.[Zn](Cl)(Cl)([Cl-])[Cl-].S(=O)(C)C
• Title of publication: Macrocyclic Rhodium(III) Hydrides and a Monomeric Rhodium(II) Complex
• Authors of publication: Andreja Bakac; Leonard M. Thomas
• Journal of publication: Inorganic Chemistry
• Year of publication: 1996
• Journal volume: 35
• Pages of publication: 5880 - 5884
• a: 10.68 ± 0.003 Å
• b: 13.46 ± 0.003 Å
• c: 14.277 ± 0.004 Å
• α: 86.49 ± 0.02°
• β: 83.18 ± 0.02°
• γ: 66.64 ± 0.02°
• Cell volume: 1870.6 ± 0.9 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1318
• Residual factor for significantly intense reflections: 0.0695
• Weighted residual factors for all reflections: 0.1857
• Weighted residual factors for significantly intense reflections: 0.1582
• Goodness-of-fit parameter for all reflections: 0.888
• Goodness-of-fit parameter for significantly intense reflections: 1.062
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No