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Information card for entry 4324725
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Coordinates | 4324725.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | N,N',N'-tris(trimethylsilyl)hydrazino-(pentafluorophenyl)chlorophosphane |
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Formula | C15 H27 Cl F5 N2 P Si3 |
Calculated formula | C15 H27 Cl F5 N2 P Si3 |
SMILES | P(Cl)(N([Si](C)(C)C)N([Si](C)(C)C)[Si](C)(C)C)c1c(F)c(F)c(F)c(F)c1F |
Title of publication | Lewis Acid Assisted Methyl/Chlorine Exchange in Silylated Hydrazinochlorophosphanes |
Authors of publication | Andrea Westenkirchner; Alexander Villinger; Konstantin Karaghiosoff; Ronald Wustrack; Dirk Michalik; Axel Schulz |
Journal of publication | Inorganic Chemistry |
Year of publication | 2011 |
Journal volume | 50 |
Pages of publication | 2691 - 2702 |
a | 15.509 ± 0.003 Å |
b | 12.823 ± 0.003 Å |
c | 11.945 ± 0.002 Å |
α | 90° |
β | 99.81 ± 0.03° |
γ | 90° |
Cell volume | 2340.8 ± 0.8 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0426 |
Residual factor for significantly intense reflections | 0.0351 |
Weighted residual factors for significantly intense reflections | 0.1026 |
Weighted residual factors for all reflections included in the refinement | 0.1076 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.077 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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