Information card for entry 4324792

Structure parameters

• Formula: C37 H54 N4 O4 Si
• Calculated formula: C37 H54 N4 O4 Si
• SMILES: c1(c(cccc1C(C)C)C(C)C)N1C(=CC(=C)N(c2c(cccc2C(C)C)C(C)C)[Si]21N(C(=O)OC(C)C)N=C(OC(C)C)O2)C
• Title of publication: Formation of Silicon Centered Spirocyclic Compounds: Reaction of N-Heterocyclic Stable Silylene with Benzoylpyridine, Diisopropyl Azodicarboxylate, and 1,2-Diphenylhydrazine
• Authors of publication: Ramachandran Azhakar; Sankaranarayana Pillai Sarish; Gašper Tavčar; Herbert W. Roesky; Jakob Hey; Dietmar Stalke; Debasis Koley
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 3028 - 3036
• a: 16.6931 ± 0.0014 Å
• b: 12.1192 ± 0.001 Å
• c: 17.9703 ± 0.0015 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3635.5 ± 0.5 ų
• Cell temperature: 99 ± 2 K
• Ambient diffraction temperature: 99 ± 2 K
• Number of distinct elements: 5
• Space group number: 29
• Hermann-Mauguin space group symbol: P c a 21
• Hall space group symbol: P 2c -2ac
• Residual factor for all reflections: 0.0322
• Residual factor for significantly intense reflections: 0.0293
• Weighted residual factors for significantly intense reflections: 0.0719
• Weighted residual factors for all reflections included in the refinement: 0.0737
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No