Information card for entry 4324875

Structure parameters

• Formula: C59 H57 O3 Os P4 Rh
• Calculated formula: C59 H57 O3 Os P4 Rh
• Title of publication: Unusual Ligand Transformations Initiated by dppm Deprotonation in Methylene-Bridged Rh/Os Complexes
• Authors of publication: Kyle D. Wells; Robert McDonald; Michael J. Ferguson; Martin Cowie
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 3523 - 3538
• a: 15.276 ± 0.002 Å
• b: 18.85 ± 0.003 Å
• c: 18.317 ± 0.002 Å
• α: 90°
• β: 93.89 ± 0.002°
• γ: 90°
• Cell volume: 5262.3 ± 1.2 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0396
• Residual factor for significantly intense reflections: 0.0332
• Weighted residual factors for significantly intense reflections: 0.0881
• Weighted residual factors for all reflections included in the refinement: 0.0969
• Goodness-of-fit parameter for all reflections included in the refinement: 1.084
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No