Information card for entry 4324876

Structure parameters

• Formula: C73 H63 O4 Os P4 Rh
• Calculated formula: C73 H63 O4 Os P4 Rh
• Title of publication: Unusual Ligand Transformations Initiated by dppm Deprotonation in Methylene-Bridged Rh/Os Complexes
• Authors of publication: Kyle D. Wells; Robert McDonald; Michael J. Ferguson; Martin Cowie
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 3523 - 3538
• a: 18.7282 ± 0.0008 Å
• b: 23.2474 ± 0.0009 Å
• c: 14.2788 ± 0.0006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6216.7 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 58
• Hermann-Mauguin space group symbol: P n n m
• Hall space group symbol: -P 2 2n
• Residual factor for all reflections: 0.0383
• Residual factor for significantly intense reflections: 0.0277
• Weighted residual factors for significantly intense reflections: 0.0654
• Weighted residual factors for all reflections included in the refinement: 0.072
• Goodness-of-fit parameter for all reflections included in the refinement: 1.058
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No