Information card for entry 4324877

Structure parameters

• Formula: C56 H47 Cl2 O4 Os P4 Rh
• Calculated formula: C56 H47 Cl2 O4 Os P4 Rh
• Title of publication: Unusual Ligand Transformations Initiated by dppm Deprotonation in Methylene-Bridged Rh/Os Complexes
• Authors of publication: Kyle D. Wells; Robert McDonald; Michael J. Ferguson; Martin Cowie
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 3523 - 3538
• a: 16.646 ± 0.0006 Å
• b: 15.387 ± 0.0006 Å
• c: 19.7962 ± 0.0007 Å
• α: 90°
• β: 90.3815 ± 0.0004°
• γ: 90°
• Cell volume: 5070.3 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0313
• Residual factor for significantly intense reflections: 0.0307
• Weighted residual factors for significantly intense reflections: 0.0672
• Weighted residual factors for all reflections included in the refinement: 0.0674
• Goodness-of-fit parameter for all reflections included in the refinement: 1.347
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No