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Information card for entry 4325211
Preview
Coordinates | 4325211.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C53 H62 Cl2 Mn2 N4 O9 Si2 |
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Calculated formula | C53 H62 Cl2 Mn2 N4 O9 Si2 |
SMILES | c1(ccccc1)C1=[N](C(C)(C)C)[Si](Cl)([Mn](C#[O])(C#[O])(C#[O])(C#[O])[Si]2(Cl)[N](=C(c3ccccc3)N2C(C)(C)C)C(C)(C)C)N1C(C)(C)C.C([Mn](C#[O])(C#[O])(C#[O])C#[O])#[O].c1(ccccc1)C.c1(ccccc1)C |
Title of publication | Syntheses of Group 7 Metal Carbonyl Complexes with a Stable N-Heterocyclic Chlorosilylene |
Authors of publication | Ramachandran Azhakar; Sankaranarayana Pillai Sarish; Herbert W. Roesky; Jakob Hey; Dietmar Stalke |
Journal of publication | Inorganic Chemistry |
Year of publication | 2011 |
Journal volume | 50 |
Pages of publication | 5039 - 5043 |
a | 8.847 ± 0.0014 Å |
b | 34.141 ± 0.005 Å |
c | 19.096 ± 0.003 Å |
α | 90° |
β | 100.555 ± 0.004° |
γ | 90° |
Cell volume | 5670.3 ± 1.5 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0582 |
Residual factor for significantly intense reflections | 0.0367 |
Weighted residual factors for significantly intense reflections | 0.0747 |
Weighted residual factors for all reflections included in the refinement | 0.0838 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.022 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4325211.html
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