Information card for entry 4325212

Structure parameters

• Formula: C60 H77 Cl3 N6 O8 Re2 Si3
• Calculated formula: C60 H77 Cl3 N6 O8 Re2 Si3
• Title of publication: Syntheses of Group 7 Metal Carbonyl Complexes with a Stable N-Heterocyclic Chlorosilylene
• Authors of publication: Ramachandran Azhakar; Sankaranarayana Pillai Sarish; Herbert W. Roesky; Jakob Hey; Dietmar Stalke
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 5039 - 5043
• a: 12.447 ± 0.0004 Å
• b: 37.801 ± 0.0013 Å
• c: 14.4401 ± 0.0005 Å
• α: 90°
• β: 90.456 ± 0.001°
• γ: 90°
• Cell volume: 6794 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0536
• Residual factor for significantly intense reflections: 0.0484
• Weighted residual factors for significantly intense reflections: 0.1074
• Weighted residual factors for all reflections included in the refinement: 0.1093
• Goodness-of-fit parameter for all reflections included in the refinement: 1.299
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No