Information card for entry 4325240

Structure parameters

• Chemical name: Uranium(IV) monoiodotetrakis(tetrahydrofuran)bistrimethylsilyloxide Triiodide
• Formula: C22 H50 I4 O6 Si2 U
• Calculated formula: C22 H25 I4 O6 Si2 U
• Title of publication: Facile Reduction of a Uranyl(VI) β-Ketoiminate Complex to U(IV) Upon Oxo Silylation
• Authors of publication: Jessie L. Brown; Charles C. Mokhtarzadeh; Jeremie M. Lever; Guang Wu; Trevor W. Hayton
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 5105 - 5112
• a: 9.519 ± 0.004 Å
• b: 12.725 ± 0.005 Å
• c: 16.355 ± 0.006 Å
• α: 89.944 ± 0.006°
• β: 74.313 ± 0.006°
• γ: 89.97 ± 0.006°
• Cell volume: 1907.3 ± 1.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0919
• Residual factor for significantly intense reflections: 0.0483
• Weighted residual factors for significantly intense reflections: 0.105
• Weighted residual factors for all reflections included in the refinement: 0.1224
• Goodness-of-fit parameter for all reflections included in the refinement: 0.973
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No