Crystallography Open Database

Information card for entry 4325517

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Coordinates	4325517.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C68 H151 N6 O28 Te V9
Calculated formula	C68 H146 N6 O28 Te V9
Title of publication	[HxTeV9O28](5-x)- (x= 1 and 2): Vanadotellurates with Decavanadate Structure
Authors of publication	Saki Konaka; Yoshiki Ozawa; Takahiro Shonaka; Shinta Watanabe; Atsushi Yagasaki
Journal of publication	Inorganic Chemistry
Year of publication	2011
Journal volume	50
Pages of publication	6183 - 6188
a	16.7102 ± 0.0006 Å
b	17.468 ± 0.0007 Å
c	17.9634 ± 0.0007 Å
α	74.412 ± 0.001°
β	67.494 ± 0.001°
γ	74.16 ± 0.002°
Cell volume	4579.9 ± 0.3 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 1 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0849
Residual factor for significantly intense reflections	0.0614
Weighted residual factors for significantly intense reflections	0.1681
Weighted residual factors for all reflections included in the refinement	0.2051
Goodness-of-fit parameter for all reflections included in the refinement	1.076
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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