Information card for entry 4325518

Structure parameters

• Formula: C106 H168 B2 Cl2 O P8 Ru2
• Calculated formula: C106 H168 B2 Cl2 O P8 Ru2
• Title of publication: Ruthenium Hydride Complexes of the Hindered Phosphine Ligand Tris(3-diisopropylphosphinopropyl)phosphine
• Authors of publication: Mohan M. Bhadbhade; Leslie D. Field; Ryan Gilbert-Wilson; Ruth W. Guest; Paul Jensen
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 6220 - 6228
• a: 12.28 ± 0.002 Å
• b: 19.093 ± 0.004 Å
• c: 23.928 ± 0.004 Å
• α: 111.889 ± 0.003°
• β: 98.687 ± 0.003°
• γ: 90.272 ± 0.003°
• Cell volume: 5134.6 ± 1.6 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0496
• Residual factor for significantly intense reflections: 0.0322
• Weighted residual factors for significantly intense reflections: 0.0754
• Weighted residual factors for all reflections included in the refinement: 0.0851
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No