Crystallography Open Database

Information card for entry 4325756

Preview

Coordinates	4325756.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C52 H189 As5 Dy4 Li8 N18 O183 W40
Calculated formula	C52 As5 Dy4 Li8 N18 O183 W40
Title of publication	Utilizing the Adaptive Polyoxometalate [As2W19O67(H2O)]14- To Support a Polynuclear Lanthanoid-Based Single-Molecule Magnet
Authors of publication	Chris Ritchie; Manfred Speldrich; Robert W. Gable; Lorenzo Sorace; Paul Kögerler; Colette Boskovic
Journal of publication	Inorganic Chemistry
Year of publication	2011
Journal volume	50
Pages of publication	7004 - 7014
a	28.7245 ± 0.0007 Å
b	25.1124 ± 0.0005 Å
c	35.1823 ± 0.001 Å
α	90°
β	110.349 ± 0.003°
γ	90°
Cell volume	23794.6 ± 1.1 Å³
Cell temperature	130 ± 2 K
Ambient diffraction temperature	130 ± 2 K
Number of distinct elements	8
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0673
Residual factor for significantly intense reflections	0.0425
Weighted residual factors for significantly intense reflections	0.1075
Weighted residual factors for all reflections included in the refinement	0.1138
Goodness-of-fit parameter for all reflections included in the refinement	0.99
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4325756.html