Crystallography Open Database

Information card for entry 4325757

Preview

Coordinates	4325757.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C52 H189 As5 Ho4 Li8 N18 O183 W40
Calculated formula	C52 As5 Ho4 Li8 N18 O183 W40
Title of publication	Utilizing the Adaptive Polyoxometalate [As2W19O67(H2O)]14- To Support a Polynuclear Lanthanoid-Based Single-Molecule Magnet
Authors of publication	Chris Ritchie; Manfred Speldrich; Robert W. Gable; Lorenzo Sorace; Paul Kögerler; Colette Boskovic
Journal of publication	Inorganic Chemistry
Year of publication	2011
Journal volume	50
Pages of publication	7004 - 7014
a	28.739 ± 0.004 Å
b	25.206 ± 0.004 Å
c	34.893 ± 0.005 Å
α	90°
β	110.184 ± 0.003°
γ	90°
Cell volume	23724 ± 6 Å³
Cell temperature	130 ± 2 K
Ambient diffraction temperature	130 ± 2 K
Number of distinct elements	8
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1315
Residual factor for significantly intense reflections	0.07
Weighted residual factors for significantly intense reflections	0.1553
Weighted residual factors for all reflections included in the refinement	0.1801
Goodness-of-fit parameter for all reflections included in the refinement	0.978
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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