Information card for entry 4325984

Structure parameters

• Formula: C64 H57 B2 F24 N O2 P2 Pd
• Calculated formula: C64 H57 B2 F24 N O2 P2 Pd
• Title of publication: Net Heterolytic Cleavage of B-H and B-B Bonds Across the N-Pd Bond in a Cationic (PNP)Pd Fragment
• Authors of publication: Yanjun Zhu; Chun-Hsing Chen; Claudia M. Fafard; Bruce M. Foxman; Oleg V. Ozerov
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 7980 - 7987
• a: 12.3756 ± 0.0009 Å
• b: 15.6639 ± 0.0011 Å
• c: 19.3865 ± 0.0014 Å
• α: 89.269 ± 0.004°
• β: 88.814 ± 0.004°
• γ: 86.015 ± 0.004°
• Cell volume: 3747.9 ± 0.5 ų
• Cell temperature: 120 K
• Ambient diffraction temperature: 120 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0712
• Residual factor for significantly intense reflections: 0.0477
• Weighted residual factors for all reflections: 0.1471
• Weighted residual factors for significantly intense reflections: 0.1237
• Weighted residual factors for all reflections included in the refinement: 0.1471
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0118
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No