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Information card for entry 4325985
Preview
Coordinates | 4325985.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C64.7 H59 B2 Cl1.4 F24 N O2.3 P2 Pd |
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Calculated formula | C64.7 H59 B2 Cl1.4 F24 N O2.3 P2 Pd |
Title of publication | Net Heterolytic Cleavage of B-H and B-B Bonds Across the N-Pd Bond in a Cationic (PNP)Pd Fragment |
Authors of publication | Yanjun Zhu; Chun-Hsing Chen; Claudia M. Fafard; Bruce M. Foxman; Oleg V. Ozerov |
Journal of publication | Inorganic Chemistry |
Year of publication | 2011 |
Journal volume | 50 |
Pages of publication | 7980 - 7987 |
a | 17.166 ± 0.0008 Å |
b | 18.3171 ± 0.0009 Å |
c | 22.9978 ± 0.0011 Å |
α | 90° |
β | 107.121 ± 0.003° |
γ | 90° |
Cell volume | 6910.8 ± 0.6 Å3 |
Cell temperature | 120 K |
Ambient diffraction temperature | 120 K |
Number of distinct elements | 9 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0775 |
Residual factor for significantly intense reflections | 0.0457 |
Weighted residual factors for all reflections | 0.1298 |
Weighted residual factors for significantly intense reflections | 0.1105 |
Weighted residual factors for all reflections included in the refinement | 0.1298 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.9765 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4325985.html
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