Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 4326202
Preview
Coordinates | 4326202.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C41 H70 F3 N6 O3 P3 S Si |
---|---|
Calculated formula | C41 H70 F3 N6 O3 P3 S Si |
Title of publication | Synthesis and Characterization of a Stable Cyclicgem-Bis(phosphaylide): a 4π-Electron Three-Membered Heterocycle |
Authors of publication | Nicola Dellus; Tsuyoshi Kato; Nathalie Saffon-Merceron; Vicenç Branchadell; Antoine Baceiredo |
Journal of publication | Inorganic Chemistry |
Year of publication | 2011 |
Journal volume | 50 |
Pages of publication | 7949 - 7951 |
a | 12.6982 ± 0.0003 Å |
b | 14.4819 ± 0.0004 Å |
c | 16.2612 ± 0.0004 Å |
α | 94.731 ± 0.002° |
β | 110.44 ± 0.001° |
γ | 105.124 ± 0.002° |
Cell volume | 2654.73 ± 0.12 Å3 |
Cell temperature | 193 ± 2 K |
Ambient diffraction temperature | 193 ± 2 K |
Number of distinct elements | 8 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1067 |
Residual factor for significantly intense reflections | 0.0753 |
Weighted residual factors for significantly intense reflections | 0.1964 |
Weighted residual factors for all reflections included in the refinement | 0.221 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.101 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4326202.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.