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Information card for entry 4326203
Preview
Coordinates | 4326203.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C42 H75 F N6 O0.5 P3 Si |
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Calculated formula | C42 H75 F N6 O0.5 P3 Si |
Title of publication | Synthesis and Characterization of a Stable Cyclicgem-Bis(phosphaylide): a 4π-Electron Three-Membered Heterocycle |
Authors of publication | Nicola Dellus; Tsuyoshi Kato; Nathalie Saffon-Merceron; Vicenç Branchadell; Antoine Baceiredo |
Journal of publication | Inorganic Chemistry |
Year of publication | 2011 |
Journal volume | 50 |
Pages of publication | 7949 - 7951 |
a | 18.6883 ± 0.0005 Å |
b | 12.2323 ± 0.0003 Å |
c | 20.8155 ± 0.0005 Å |
α | 90° |
β | 94.715 ± 0.001° |
γ | 90° |
Cell volume | 4742.3 ± 0.2 Å3 |
Cell temperature | 193 ± 2 K |
Ambient diffraction temperature | 193 ± 2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0797 |
Residual factor for significantly intense reflections | 0.0487 |
Weighted residual factors for significantly intense reflections | 0.121 |
Weighted residual factors for all reflections included in the refinement | 0.14 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.024 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4326203.html
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