Information card for entry 4326256

Structure parameters

• Formula: C43 H49 F24 N8 O4 Os2 P4
• Calculated formula: C43 H48 F24 N8 O4 Os2 P4
• SMILES: [Os]1234(O[Os]567([O]=C(O1)CCC)[N](Cc1[n]5cccc1)(Cc1[n]6cccc1)Cc1[n]7cccc1)[N](Cc1[n]2cccc1)(Cc1[n]3cccc1)Cc1[n]4cccc1.[P](F)(F)(F)(F)(F)[F-].[P](F)(F)(F)(F)(F)[F-].[P](F)(F)(F)(F)(F)[F-].[P](F)(F)(F)(F)(F)[F-].O=C(C)C
• Title of publication: Synthesis and Properties of Oxo-carboxylato- and Dioxo-Bridged Diosmium Complexes of Tris(2-pyridylmethyl)amine
• Authors of publication: Hideki Sugimoto; Kazuhiro Kitayama; Kenji Ashikari; Chikako Matsunami; Naomi Ueda; Keisuke Umakoshi; Yuko Hosokoshi; Yoichi Sasaki; Shinobu Itoh
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 9014 - 9023
• a: 19.587 ± 0.007 Å
• b: 12.304 ± 0.005 Å
• c: 23.333 ± 0.008 Å
• α: 90°
• β: 91.838 ± 0.004°
• γ: 90°
• Cell volume: 5620 ± 4 ų
• Cell temperature: 113 K
• Ambient diffraction temperature: 113 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 0.0648
• Weighted residual factors for all reflections included in the refinement: 0.1611
• Goodness-of-fit parameter for all reflections included in the refinement: 0.787
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No