Information card for entry 4327313

Structure parameters

• Formula: C40 H58 N4 O V
• Calculated formula: C43 H64 N4 O V
• Title of publication: Dinitrogen Partial Reduction by Formally Zero- and Divalent Vanadium Complexes Supported by the Bis-iminopyridine System
• Authors of publication: Indu Vidyaratne; Sandro Gambarotta; Ilia Korobkov; Peter H. M. Budzelaar
• Journal of publication: Inorganic Chemistry
• Year of publication: 2005
• Journal volume: 44
• Pages of publication: 1187 - 1189
• a: 25.401 ± 0.002 Å
• b: 11.6983 ± 0.0011 Å
• c: 30.425 ± 0.003 Å
• α: 90°
• β: 113.643 ± 0.002°
• γ: 90°
• Cell volume: 8281.9 ± 1.3 ų
• Cell temperature: 206 ± 2 K
• Ambient diffraction temperature: 206 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1107
• Residual factor for significantly intense reflections: 0.0658
• Weighted residual factors for significantly intense reflections: 0.142
• Weighted residual factors for all reflections included in the refinement: 0.1575
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No