Information card for entry 4327314

Structure parameters

• Formula: C40 H56 N4 O V
• Calculated formula: C37 H49 N4 O V
• Title of publication: Dinitrogen Partial Reduction by Formally Zero- and Divalent Vanadium Complexes Supported by the Bis-iminopyridine System
• Authors of publication: Indu Vidyaratne; Sandro Gambarotta; Ilia Korobkov; Peter H. M. Budzelaar
• Journal of publication: Inorganic Chemistry
• Year of publication: 2005
• Journal volume: 44
• Pages of publication: 1187 - 1189
• a: 25.093 ± 0.004 Å
• b: 11.7898 ± 0.0018 Å
• c: 30.183 ± 0.005 Å
• α: 90°
• β: 112.754 ± 0.003°
• γ: 90°
• Cell volume: 8234 ± 2 ų
• Cell temperature: 208 ± 2 K
• Ambient diffraction temperature: 208 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0999
• Residual factor for significantly intense reflections: 0.0634
• Weighted residual factors for significantly intense reflections: 0.1568
• Weighted residual factors for all reflections included in the refinement: 0.1714
• Goodness-of-fit parameter for all reflections included in the refinement: 1.004
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No