Crystallography Open Database

Information card for entry 4327653

Preview

Coordinates	4327653.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H38 Br3 Mo3 N O10 P3 S9 Sb
Calculated formula	C22 H38 Br3 Mo3 N O10 P3 S9 Sb
Title of publication	Synthesis, Crystal Structure, and Spectroscopic Characterization of a Series of Cubane-like Mo-Sb Clusters Containing a [Mo3SbOS3]7+ Core
Authors of publication	Shao-Fang Lu; Jian-Quan Huang; Xiao-Ying Huang; Qiang-Jin Wu; Rong-Min Yu
Journal of publication	Inorganic Chemistry
Year of publication	1999
Journal volume	38
Pages of publication	3801 - 3805
a	12.758 ± 0.014 Å
b	17.859 ± 0.013 Å
c	11.882 ± 0.004 Å
α	75.05 ± 0.04°
β	88.15 ± 0.07°
γ	73.24 ± 0.07°
Cell volume	2502 ± 4 Å³
Cell temperature	293 K
Number of distinct elements	9
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for significantly intense reflections	0.086
Weighted residual factors for significantly intense reflections	0.099
Goodness-of-fit parameter for significantly intense reflections	1.65
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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