Crystallography Open Database

Information card for entry 4327654

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Coordinates	4327654.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H44 I3 Mo3 N O10 P3 S9 Sb
Calculated formula	C22.1667 H38 I3 Mo3 N O9.875 P3 S9 Sb
Title of publication	Synthesis, Crystal Structure, and Spectroscopic Characterization of a Series of Cubane-like Mo-Sb Clusters Containing a [Mo3SbOS3]7+ Core
Authors of publication	Shao-Fang Lu; Jian-Quan Huang; Xiao-Ying Huang; Qiang-Jin Wu; Rong-Min Yu
Journal of publication	Inorganic Chemistry
Year of publication	1999
Journal volume	38
Pages of publication	3801 - 3805
a	11.727 ± 0.005 Å
b	12.951 ± 0.003 Å
c	17.957 ± 0.004 Å
α	73.52 ± 0.03°
β	76.22 ± 0.03°
γ	89 ± 0.03°
Cell volume	2536.3 ± 1.5 Å³
Cell temperature	293 K
Number of distinct elements	9
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for significantly intense reflections	0.053
Weighted residual factors for significantly intense reflections	0.065
Goodness-of-fit parameter for significantly intense reflections	1.44
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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