Crystallography Open Database

Information card for entry 4327655

Preview

Coordinates	4327655.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C18 H33.5 Br3 Mo3 N O9.5 P2 S7 Sb
Calculated formula	C18 H31 Br3 Mo3 N O9.5 P2 S7 Sb
Title of publication	Synthesis, Crystal Structure, and Spectroscopic Characterization of a Series of Cubane-like Mo-Sb Clusters Containing a [Mo3SbOS3]7+ Core
Authors of publication	Shao-Fang Lu; Jian-Quan Huang; Xiao-Ying Huang; Qiang-Jin Wu; Rong-Min Yu
Journal of publication	Inorganic Chemistry
Year of publication	1999
Journal volume	38
Pages of publication	3801 - 3805
a	13.261 ± 0.004 Å
b	13.529 ± 0.004 Å
c	12.535 ± 0.008 Å
α	101.54 ± 0.03°
β	105.13 ± 0.04°
γ	93.2 ± 0.02°
Cell volume	2113.1 ± 1.7 Å³
Cell temperature	293 K
Number of distinct elements	9
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for significantly intense reflections	0.06
Weighted residual factors for significantly intense reflections	0.076
Goodness-of-fit parameter for significantly intense reflections	1.65
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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