Information card for entry 4327708

Structure parameters

• Formula: C65 H93 F P2 Si2
• Calculated formula: C64.98 H92.94 F P2 Si2
• Title of publication: A Facile Synthesis of Diphosphasilacyclopropanes and 1,3-Diphospha-2,4-disilabicyclo[1.1.0]butanes and an ab Initio Study of Diphosphadisilabicyclo[1.1.0]butanes and Their Respective 1,3-Diene Isomers
• Authors of publication: Matthias Driess; Hans Pritzkow; Stefan Rell; Rudolf Janoschek
• Journal of publication: Inorganic Chemistry
• Year of publication: 1997
• Journal volume: 36
• Pages of publication: 5212 - 5217
• a: 14.847 ± 0.003 Å
• b: 22.559 ± 0.005 Å
• c: 21.071 ± 0.003 Å
• α: 90°
• β: 77.74 ± 0.01°
• γ: 90°
• Cell volume: 6896 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1847
• Residual factor for significantly intense reflections: 0.0859
• Weighted residual factors for all reflections: 0.2704
• Weighted residual factors for significantly intense reflections: 0.2062
• Goodness-of-fit parameter for all reflections: 1.035
• Goodness-of-fit parameter for significantly intense reflections: 1.165
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No