Information card for entry 4327709

Structure parameters

• Formula: C77 H123 F Li O3 P2 Si2
• Calculated formula: C77 H123 F Li O3 P2 Si2
• Title of publication: A Facile Synthesis of Diphosphasilacyclopropanes and 1,3-Diphospha-2,4-disilabicyclo[1.1.0]butanes and an ab Initio Study of Diphosphadisilabicyclo[1.1.0]butanes and Their Respective 1,3-Diene Isomers
• Authors of publication: Matthias Driess; Hans Pritzkow; Stefan Rell; Rudolf Janoschek
• Journal of publication: Inorganic Chemistry
• Year of publication: 1997
• Journal volume: 36
• Pages of publication: 5212 - 5217
• a: 14.845 ± 0.011 Å
• b: 24.594 ± 0.019 Å
• c: 21.132 ± 0.016 Å
• α: 90°
• β: 93.88 ± 0.06°
• γ: 90°
• Cell volume: 7698 ± 10 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1832
• Residual factor for significantly intense reflections: 0.0767
• Weighted residual factors for all reflections: 0.2064
• Weighted residual factors for significantly intense reflections: 0.159
• Goodness-of-fit parameter for all reflections: 1.022
• Goodness-of-fit parameter for significantly intense reflections: 1.134
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No