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Information card for entry 4327966
Preview
Coordinates | 4327966.cif |
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Original paper (by DOI) | HTML |
Formula | C28 H30 N2 P2 |
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Calculated formula | C28 H30 N2 P2 |
SMILES | P(N(P(c1ccccc1)c1ccccc1)NC(C)(C)C)(c1ccccc1)c1ccccc1 |
Title of publication | The Intramolecular Rearrangement of Phosphinohydrazides [R'2P-NR-NR-M] →[RN=PR'2-NR-M]: General Rules and Exceptions. Transformations of Bulky Phosphinohydrazines (R-NH-N(PPh2)2, R =tBu, Ph2P) |
Authors of publication | Alexander N. Kornev; Vyacheslav V. Sushev; Yulia S. Panova; Natalia V. Belina; Olga V. Lukoyanova; Georgy K. Fukin; Sergey Y. Ketkov; Gleb A. Abakumov; Peter Lönnecke; Evamarie Hey-Hawkins |
Journal of publication | Inorganic Chemistry |
Year of publication | 2012 |
Journal volume | 51 |
Pages of publication | 874 - 881 |
a | 12.2853 ± 0.0002 Å |
b | 31.6711 ± 0.0005 Å |
c | 12.8947 ± 0.0003 Å |
α | 90° |
β | 90.036 ± 0.002° |
γ | 90° |
Cell volume | 5017.18 ± 0.16 Å3 |
Cell temperature | 130 ± 2 K |
Ambient diffraction temperature | 130 ± 2 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0841 |
Residual factor for significantly intense reflections | 0.0592 |
Weighted residual factors for significantly intense reflections | 0.1485 |
Weighted residual factors for all reflections included in the refinement | 0.1559 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.19 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4327966.html
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Users of the data should acknowledge the original authors of the
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