Information card for entry 4329821

Structure parameters

• Formula: C33 H48 Ge N3 P
• Calculated formula: C33 H48 Ge N3 P
• SMILES: [Ge]1([P]2(N(C(C)C)CCN2C(C)C)C2=C(N1c1c(cccc1C(C)C)C(C)C)[C@@H]1CC[C@H]2C1)c1ccccc1.[Ge]1([P]2(N(C(C)C)CCN2C(C)C)C2=C(N1c1c(cccc1C(C)C)C(C)C)[C@H]1CC[C@@H]2C1)c1ccccc1
• Title of publication: Synthesis and Characterization of Rhodium Complexes with Phosphine-Stabilized Germylenes
• Authors of publication: Juan Manuel García; Edgar Ocando Mavárez; Tsuyoshi Kato; David Santiago Coll; Alexander Briceño; Nathalie Saffon-Merceron; Antoine Bacereido
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 8187 - 8193
• a: 18.7398 ± 0.0003 Å
• b: 16.2976 ± 0.0002 Å
• c: 10.7861 ± 0.0002 Å
• α: 90°
• β: 101.61 ± 0.001°
• γ: 90°
• Cell volume: 3226.82 ± 0.09 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0589
• Residual factor for significantly intense reflections: 0.0363
• Weighted residual factors for significantly intense reflections: 0.0815
• Weighted residual factors for all reflections included in the refinement: 0.0908
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No