Information card for entry 4329836

Structure parameters

• Chemical name: N-(trifluoromethylsulfonyl)dimethylsilyl-N-[2,6-bis(2,4,6-trimethylphenyl) phenyl]amino-chloro-methylstibane
• Formula: C28 H34 Cl F3 N O3 S Sb Si
• Calculated formula: C28 H34 Cl F3 N O3 S Sb Si
• SMILES: [Sb](Cl)(N([Si](OS(=O)(=O)C(F)(F)F)(C)C)c1c(cccc1c1c(cc(cc1C)C)C)c1c(cc(cc1C)C)C)C
• Title of publication: Chlorine/Methyl Exchange Reactions in Silylated Aminostibanes: A New Route To Stibinostibonium Cations
• Authors of publication: Christian Hering; Mathias Lehmann; Axel Schulz; Alexander Villinger
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 8212 - 8224
• a: 21.987 ± 0.009 Å
• b: 9.225 ± 0.004 Å
• c: 16.128 ± 0.008 Å
• α: 90°
• β: 109.841 ± 0.013°
• γ: 90°
• Cell volume: 3077 ± 2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 9
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0556
• Residual factor for significantly intense reflections: 0.0395
• Weighted residual factors for significantly intense reflections: 0.0986
• Weighted residual factors for all reflections included in the refinement: 0.1039
• Goodness-of-fit parameter for all reflections included in the refinement: 1.058
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No