Information card for entry 4329963

Structure parameters

• Formula: C14 H38 Cl14 N4 Si6
• Calculated formula: C14 H38 Cl14 N4 Si6
• SMILES: C(C[N+](C)(C)C)N(C)C.[Cl-].[Si]1([Si]([Si](Cl)([Si]([Si]([Si]1(Cl)Cl)(Cl)Cl)(Cl)Cl)Cl)(Cl)Cl)(Cl)Cl.C(C[N+](C)(C)C)N(C)C.[Cl-]
• Title of publication: Unexpected Disproportionation of Tetramethylethylenediamine-Supported Perchlorodisilane Cl3SiSiCl3
• Authors of publication: Jan Tillmann; Frank Meyer-Wegner; Andor Nadj; Johanna Becker-Baldus; Tanja Sinke; Michael Bolte; Max C. Holthausen; Matthias Wagner; Hans-Wolfram Lerner
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 8599 - 8606
• a: 10.163 ± 0.0008 Å
• b: 10.4876 ± 0.001 Å
• c: 18.4868 ± 0.0016 Å
• α: 90°
• β: 98.913 ± 0.007°
• γ: 90°
• Cell volume: 1946.6 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0991
• Residual factor for significantly intense reflections: 0.0729
• Weighted residual factors for significantly intense reflections: 0.1158
• Weighted residual factors for all reflections included in the refinement: 0.1235
• Goodness-of-fit parameter for all reflections included in the refinement: 1.148
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No