Information card for entry 4329964

Structure parameters

• Formula: C6 H16 Cl4 N2 Si
• Calculated formula: C6 H16 Cl4 N2 Si
• SMILES: [Si]1(Cl)(Cl)(Cl)(Cl)[N](CC[N]1(C)C)(C)C
• Title of publication: Unexpected Disproportionation of Tetramethylethylenediamine-Supported Perchlorodisilane Cl3SiSiCl3
• Authors of publication: Jan Tillmann; Frank Meyer-Wegner; Andor Nadj; Johanna Becker-Baldus; Tanja Sinke; Michael Bolte; Max C. Holthausen; Matthias Wagner; Hans-Wolfram Lerner
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 8599 - 8606
• a: 23.2626 ± 0.0013 Å
• b: 14.4338 ± 0.0007 Å
• c: 14.3613 ± 0.0008 Å
• α: 90°
• β: 92.825 ± 0.005°
• γ: 90°
• Cell volume: 4816.2 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0964
• Residual factor for significantly intense reflections: 0.0918
• Weighted residual factors for significantly intense reflections: 0.2194
• Weighted residual factors for all reflections included in the refinement: 0.221
• Goodness-of-fit parameter for all reflections included in the refinement: 1.988
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No