Information card for entry 4330128

Structure parameters

• Formula: C105 H102 Cl Co4 N16 O22.72 P3
• Calculated formula: C105 H102 Cl Co4 N16 O22.715 P3
• Title of publication: Enantioselective Synthesis of Tetranuclear Quadruple Helicates
• Authors of publication: Claire Deville; Alexandra Spyratou; Paulina Aguirre-Etcheverry; Céline Besnard; Alan F. Williams
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 8667 - 8669
• a: 13.4175 ± 0.0003 Å
• b: 15.4982 ± 0.0006 Å
• c: 52.7507 ± 0.0017 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 10969.4 ± 0.6 ų
• Cell temperature: 180 K
• Ambient diffraction temperature: 180 K
• Number of distinct elements: 7
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0804
• Residual factor for significantly intense reflections: 0.0634
• Weighted residual factors for significantly intense reflections: 0.1628
• Weighted residual factors for all reflections included in the refinement: 0.1749
• Goodness-of-fit parameter for all reflections included in the refinement: 1.071
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No