Crystallography Open Database

Information card for entry 4330129

Preview

Coordinates	4330129.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C119.35 H121.4 Co4 N16 O19.85 P4
Calculated formula	C119.347 H121.388 Co4 N16 O19.847 P4
Title of publication	Enantioselective Synthesis of Tetranuclear Quadruple Helicates
Authors of publication	Claire Deville; Alexandra Spyratou; Paulina Aguirre-Etcheverry; Céline Besnard; Alan F. Williams
Journal of publication	Inorganic Chemistry
Year of publication	2012
Journal volume	51
Pages of publication	8667 - 8669
a	16.5412 ± 0.0005 Å
b	19.2351 ± 0.0005 Å
c	19.8514 ± 0.0005 Å
α	97.666 ± 0.002°
β	91.277 ± 0.002°
γ	108.58 ± 0.003°
Cell volume	5919.3 ± 0.3 Å³
Cell temperature	159.6 K
Ambient diffraction temperature	159.6 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0731
Residual factor for significantly intense reflections	0.0667
Weighted residual factors for significantly intense reflections	0.1931
Weighted residual factors for all reflections included in the refinement	0.202
Goodness-of-fit parameter for all reflections included in the refinement	1.03
Diffraction radiation wavelength	1.5418 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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