Crystallography Open Database

Information card for entry 4330130

Preview

Coordinates	4330130.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C83.68 H96.93 Co4 N16 O17.29
Calculated formula	C83.672 H96.902 Co4 N16 O17.514
Title of publication	Enantioselective Synthesis of Tetranuclear Quadruple Helicates
Authors of publication	Claire Deville; Alexandra Spyratou; Paulina Aguirre-Etcheverry; Céline Besnard; Alan F. Williams
Journal of publication	Inorganic Chemistry
Year of publication	2012
Journal volume	51
Pages of publication	8667 - 8669
a	10.72917 ± 0.00011 Å
b	25.2968 ± 0.0003 Å
c	17.3108 ± 0.0002 Å
α	90°
β	94.5232 ± 0.001°
γ	90°
Cell volume	4683.75 ± 0.09 Å³
Cell temperature	179.9 K
Ambient diffraction temperature	179.9 K
Number of distinct elements	5
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.0569
Residual factor for significantly intense reflections	0.0544
Weighted residual factors for significantly intense reflections	0.1442
Weighted residual factors for all reflections included in the refinement	0.147
Goodness-of-fit parameter for all reflections included in the refinement	1.028
Diffraction radiation wavelength	1.5418 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4330130.html