Information card for entry 4330135

Structure parameters

• Formula: C117 H95 Au5 N O19 P5 Rh10
• Calculated formula: C114 H87 Au5 N O18 P5 Rh10
• Title of publication: Synthesis, Reactivity, Electrochemical Behavior, and Crystal Structure of a Family of Multivalent Metal Carbido-Carbonyl Clusters Based on the Rh10(C)2Au4-6Framework
• Authors of publication: Laura Cherchi; Alessandro Fumagalli; Serena Fedi; Piero Zanello; Fabrizia Fabrizi De Biani; Franco Laschi; Luigi Garlaschelli; Piero Macchi; Angelo Sironi
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 9171 - 9180
• a: 14.862 ± 0.007 Å
• b: 17.39 ± 0.009 Å
• c: 24.298 ± 0.012 Å
• α: 88.542 ± 0.008°
• β: 87.651 ± 0.008°
• γ: 84.051 ± 0.008°
• Cell volume: 6239 ± 5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.16
• Residual factor for significantly intense reflections: 0.1034
• Weighted residual factors for significantly intense reflections: 0.2444
• Weighted residual factors for all reflections included in the refinement: 0.2678
• Goodness-of-fit parameter for all reflections included in the refinement: 1.104
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No