Information card for entry 4331236

Structure parameters

• Formula: C48 H67 Al Li N O3 Si
• Calculated formula: C48 H67 Al Li N O3 Si
• SMILES: [Si](N([AlH2][H][Li]([O]1CCCC1)([O](CC)CC)[O](CC)CC)c1c(cc(cc1C(c1ccccc1)c1ccccc1)C)C(c1ccccc1)c1ccccc1)(C)(C)C
• Title of publication: Monomeric Group 13 Metal(I) Amides: Enforcing One-Coordination Through Extreme Ligand Steric Bulk
• Authors of publication: Deepak Dange; Jiaye Li; Christian Schenk; Hansgeorg Schnöckel; Cameron Jones
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 13050 - 13059
• a: 12.9536 ± 0.0003 Å
• b: 25.9791 ± 0.0006 Å
• c: 13.7056 ± 0.0004 Å
• α: 90°
• β: 97.686 ± 0.002°
• γ: 90°
• Cell volume: 4570.8 ± 0.2 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0836
• Residual factor for significantly intense reflections: 0.0583
• Weighted residual factors for significantly intense reflections: 0.1477
• Weighted residual factors for all reflections included in the refinement: 0.1644
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No