Information card for entry 4331237

Structure parameters

• Formula: C86 H94 Al2 K2 N2 Si2
• Calculated formula: C86 H94 Al2 K2 N2 Si2
• SMILES: c1(c(cc(cc1C(c1ccccc1)c1ccccc1)C)C(c1ccccc1)c1ccccc1)N([AlH3])[Si](C)(C)C.[K+].c1(ccccc1)C
• Title of publication: Monomeric Group 13 Metal(I) Amides: Enforcing One-Coordination Through Extreme Ligand Steric Bulk
• Authors of publication: Deepak Dange; Jiaye Li; Christian Schenk; Hansgeorg Schnöckel; Cameron Jones
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 13050 - 13059
• a: 10.2955 ± 0.0005 Å
• b: 12.6163 ± 0.0007 Å
• c: 15.1988 ± 0.0007 Å
• α: 100.176 ± 0.004°
• β: 99.877 ± 0.004°
• γ: 91.641 ± 0.004°
• Cell volume: 1910.79 ± 0.17 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0671
• Residual factor for significantly intense reflections: 0.0479
• Weighted residual factors for significantly intense reflections: 0.1102
• Weighted residual factors for all reflections included in the refinement: 0.1253
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No