Information card for entry 4333620

Structure parameters

• Formula: Co2 H50 K12 O91 Si2 W18
• Calculated formula: Co2 H10 K12 O91 Si2 W18
• Title of publication: Di- and Tri-Cobalt Silicotungstates: Synthesis, Characterization, and Stability Studies
• Authors of publication: Guibo Zhu; Yurii V. Geletii; Jie Song; Chongchao Zhao; Elliot N. Glass; John Bacsa; Craig L. Hill
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 1018 - 1024
• a: 12.2891 ± 0.0003 Å
• b: 23.5596 ± 0.0005 Å
• c: 30.7185 ± 0.0007 Å
• α: 90°
• β: 95.88 ± 0.001°
• γ: 90°
• Cell volume: 8847 ± 0.4 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 110 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0592
• Residual factor for significantly intense reflections: 0.0482
• Weighted residual factors for significantly intense reflections: 0.1104
• Weighted residual factors for all reflections included in the refinement: 0.1154
• Goodness-of-fit parameter for all reflections included in the refinement: 1.085
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No