Information card for entry 4333619

Structure parameters

• Formula: Co3 H62 K6 Na4 O97 Si2 W18
• Calculated formula: Co3 K6 Na4 O89.8 Si2 W18
• Title of publication: Di- and Tri-Cobalt Silicotungstates: Synthesis, Characterization, and Stability Studies
• Authors of publication: Guibo Zhu; Yurii V. Geletii; Jie Song; Chongchao Zhao; Elliot N. Glass; John Bacsa; Craig L. Hill
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 1018 - 1024
• a: 13.3935 ± 0.0012 Å
• b: 16.1715 ± 0.0015 Å
• c: 20.3596 ± 0.0018 Å
• α: 90°
• β: 106.364 ± 0.001°
• γ: 90°
• Cell volume: 4231.1 ± 0.7 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 11
• Hermann-Mauguin space group symbol: P 1 21/m 1
• Hall space group symbol: -P 2yb
• Residual factor for all reflections: 0.0952
• Residual factor for significantly intense reflections: 0.0487
• Weighted residual factors for significantly intense reflections: 0.1025
• Weighted residual factors for all reflections included in the refinement: 0.1212
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No