Information card for entry 4334045

Structure parameters

• Formula: C162 Cl20 N8 O80 Pd4 Si2 W20
• Calculated formula: C162 Cl20 N8 O80 Pd4 Si2 W20
• Title of publication: Synthesis and Structural Characterization of Inorganic-Organic-Inorganic Hybrids of Dipalladium-Substituted γ-Keggin Silicodecatungstates
• Authors of publication: Tomohisa Hirano; Kazuhiro Uehara; Sayaka Uchida; Mitsuhiro Hibino; Keigo Kamata; Noritaka Mizuno
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 2662 - 2670
• a: 29.4889 ± 0.0009 Å
• b: 28.588 ± 0.0006 Å
• c: 29.7538 ± 0.0008 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 25083.3 ± 1.1 ų
• Cell temperature: 123 K
• Ambient diffraction temperature: 123 K
• Number of distinct elements: 7
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for significantly intense reflections: 0.103
• Weighted residual factors for all reflections included in the refinement: 0.3242
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No