Crystallography Open Database

Information card for entry 4334046

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Coordinates	4334046.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C134 N8 O80 Pd4 Si2 W20
Calculated formula	C134 N8 O80 Pd4 Si2 W20
Title of publication	Synthesis and Structural Characterization of Inorganic-Organic-Inorganic Hybrids of Dipalladium-Substituted γ-Keggin Silicodecatungstates
Authors of publication	Tomohisa Hirano; Kazuhiro Uehara; Sayaka Uchida; Mitsuhiro Hibino; Keigo Kamata; Noritaka Mizuno
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	2662 - 2670
a	17.0069 ± 0.0002 Å
b	24.7919 ± 0.0003 Å
c	27.3714 ± 0.0004 Å
α	90°
β	92.608 ± 0.001°
γ	90°
Cell volume	11528.7 ± 0.3 Å³
Cell temperature	183 K
Ambient diffraction temperature	183 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/a 1
Hall space group symbol	-P 2yab
Residual factor for significantly intense reflections	0.0726
Weighted residual factors for all reflections included in the refinement	0.2427
Goodness-of-fit parameter for all reflections included in the refinement	1.112
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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