Information card for entry 4334047

Structure parameters

• Formula: C140 Cl2 N8 O80 Pd4 Si2 V0 W20
• Calculated formula: C140.004 Cl2 N8 O80 Pd4 Si2 W20
• Title of publication: Synthesis and Structural Characterization of Inorganic-Organic-Inorganic Hybrids of Dipalladium-Substituted γ-Keggin Silicodecatungstates
• Authors of publication: Tomohisa Hirano; Kazuhiro Uehara; Sayaka Uchida; Mitsuhiro Hibino; Keigo Kamata; Noritaka Mizuno
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 2662 - 2670
• a: 30.4333 ± 0.0002 Å
• b: 26.6216 ± 0.0002 Å
• c: 31.2528 ± 0.0002 Å
• α: 90°
• β: 112.714 ± 0.0003°
• γ: 90°
• Cell volume: 23356.7 ± 0.3 ų
• Cell temperature: 153 K
• Ambient diffraction temperature: 153 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/a 1
• Hall space group symbol: -P 2yab
• Residual factor for significantly intense reflections: 0.0809
• Weighted residual factors for all reflections included in the refinement: 0.2746
• Goodness-of-fit parameter for all reflections included in the refinement: 1.163
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No