Information card for entry 4334324

Structure parameters

• Formula: C80 H88 Br2 Fe2 N2 O2 Si2
• Calculated formula: C80 H88 Br2 Fe2 N2 O2 Si2
• Title of publication: Extremely Bulky Amido First Row Transition Metal(II) Halide Complexes: Potential Precursors to Low Coordinate Metal-Metal Bonded Systems
• Authors of publication: Jamie Hicks; Cameron Jones
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 3900 - 3907
• a: 16.4622 ± 0.0014 Å
• b: 12.6193 ± 0.0007 Å
• c: 18.6176 ± 0.0014 Å
• α: 90°
• β: 114.497 ± 0.01°
• γ: 90°
• Cell volume: 3519.5 ± 0.5 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0592
• Residual factor for significantly intense reflections: 0.0451
• Weighted residual factors for significantly intense reflections: 0.1073
• Weighted residual factors for all reflections included in the refinement: 0.1187
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No