Information card for entry 4334325

Structure parameters

• Formula: C129.8 H131.2 Br2 Fe2 N2 O2 Si2
• Calculated formula: C129.8 H131.2 Br2 Fe2 N2 O2 Si2
• Title of publication: Extremely Bulky Amido First Row Transition Metal(II) Halide Complexes: Potential Precursors to Low Coordinate Metal-Metal Bonded Systems
• Authors of publication: Jamie Hicks; Cameron Jones
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 3900 - 3907
• a: 14.0504 ± 0.0004 Å
• b: 14.5583 ± 0.0005 Å
• c: 15.2887 ± 0.0005 Å
• α: 64.52 ± 0.003°
• β: 70.367 ± 0.003°
• γ: 78.91 ± 0.003°
• Cell volume: 2654.8 ± 0.17 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0406
• Residual factor for significantly intense reflections: 0.0318
• Weighted residual factors for significantly intense reflections: 0.0766
• Weighted residual factors for all reflections included in the refinement: 0.082
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No