Information card for entry 4334675

Structure parameters

• Chemical name: N,N-bis(trimethylsilyl)amino(isocyanato)phosphenium tetrachlorogallate
• Formula: C7 H18 Cl4 Ga N2 O P Si2
• Calculated formula: C7 H18 Cl4 Ga N2 O P Si2
• Title of publication: On the Synthesis and Reactivity of Highly Labile Pseudohalogen Phosphenium Ions
• Authors of publication: Christian Hering; Axel Schulz; Alexander Villinger
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 5214 - 5225
• a: 10.1628 ± 0.0002 Å
• b: 11.9467 ± 0.0003 Å
• c: 15.8593 ± 0.0004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1925.51 ± 0.08 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0253
• Residual factor for significantly intense reflections: 0.0212
• Weighted residual factors for significantly intense reflections: 0.05
• Weighted residual factors for all reflections included in the refinement: 0.0511
• Goodness-of-fit parameter for all reflections included in the refinement: 1.012
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No