Information card for entry 4334686

Structure parameters

• Formula: C15.5 H30 Cl4 Ga N4 P Si2
• Calculated formula: C15.5 H30 Cl4 Ga N4 P Si2
• Title of publication: On the Synthesis and Reactivity of Highly Labile Pseudohalogen Phosphenium Ions
• Authors of publication: Christian Hering; Axel Schulz; Alexander Villinger
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 5214 - 5225
• a: 9.1605 ± 0.0006 Å
• b: 10.0806 ± 0.0008 Å
• c: 14.5753 ± 0.0011 Å
• α: 97.471 ± 0.004°
• β: 96.939 ± 0.004°
• γ: 94.922 ± 0.004°
• Cell volume: 1317.67 ± 0.17 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0714
• Residual factor for significantly intense reflections: 0.0388
• Weighted residual factors for significantly intense reflections: 0.0802
• Weighted residual factors for all reflections included in the refinement: 0.0933
• Goodness-of-fit parameter for all reflections included in the refinement: 1.015
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No