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Information card for entry 4334687
Preview
Coordinates | 4334687.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C13 H28 Cl4 Ga N2 O P Si2 |
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Calculated formula | C13 H28 Cl4 Ga N2 O P Si2 |
SMILES | [P+]1(N=C=O)(N([Si](C)(C)C)[Si](C)(C)C)CC(=C(C1)C)C.[Ga]([Cl-])(Cl)(Cl)Cl |
Title of publication | On the Synthesis and Reactivity of Highly Labile Pseudohalogen Phosphenium Ions |
Authors of publication | Christian Hering; Axel Schulz; Alexander Villinger |
Journal of publication | Inorganic Chemistry |
Year of publication | 2013 |
Journal volume | 52 |
Pages of publication | 5214 - 5225 |
a | 10.2146 ± 0.0002 Å |
b | 19.1054 ± 0.0004 Å |
c | 12.4856 ± 0.0002 Å |
α | 90° |
β | 102.884 ± 0.001° |
γ | 90° |
Cell volume | 2375.27 ± 0.08 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 8 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0731 |
Residual factor for significantly intense reflections | 0.0364 |
Weighted residual factors for significantly intense reflections | 0.0661 |
Weighted residual factors for all reflections included in the refinement | 0.0756 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.019 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4334687.html
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