Crystallography Open Database

Information card for entry 4335186

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Coordinates	4335186.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C21 H24 Cl8 N4 Ru
Calculated formula	C21 H24 Cl8 N4 Ru
Title of publication	Tri(pyridylmethyl)phosphine: The Elusive Congener of TPA Shows Surprisingly Different Coordination Behavior
Authors of publication	Christopher J. Whiteoak; James D. Nobbs; Evgeny Kiryushchenkov; Sandro Pagano; Andrew J.P. White; George J.P. Britovsek
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	7000 - 7009
a	8.54332 ± 0.0001 Å
b	24.0817 ± 0.0003 Å
c	13.86264 ± 0.00017 Å
α	90°
β	96.5352 ± 0.0011°
γ	90°
Cell volume	2833.53 ± 0.06 Å³
Cell temperature	173 K
Ambient diffraction temperature	173 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0474
Residual factor for significantly intense reflections	0.0359
Weighted residual factors for significantly intense reflections	0.0749
Weighted residual factors for all reflections included in the refinement	0.0767
Goodness-of-fit parameter for all reflections included in the refinement	1.126
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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